Installation and calibration of a new device for studying the thermal desorption of hydrogen isotopes from materials
Thermal desorption spectroscopy is a method typically used in surface science to study the kinematics of desorbing species from a material. Typically the sample is heated in a linear heating rate and the desorbing species are detected by a mass spectrometer during the heating. The candidate would build the set-up, calibrate the mass spectrometer to gain absolute amounts of desorbing species. Once the set-up would be commissioned the candidate would study hydrogen desorption from materials like tungsten where our group has a lot of experience.
de Jong, A.M., Niemantsverdriet, J.W., 1990. Thermal desorption analysis: Comparative test of ten commonly applied procedures. Surface Science 233, 355–365. link
Salançon, E., Dürbeck, T., Schwarz-Selinger, T., Genoese, F., Jacob, W., 2008. Redeposition of amorphous hydrogenated carbon films during thermal decomposition. Journal of Nuclear Materials 376, 160–168. link
Wang, P., Jacob, W., Gao, L., Dürbeck, T., Schwarz-Selinger, T., 2013. Comparing deuterium retention in tungsten films measured by temperature programmed desorption and nuclear reaction analysis. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms 300, 54–61. link